ANSI/ASTM D6443-2004 用波长散射X射线荧光光谱法测定未用过的润滑油和添加剂中的钙、氯、铜、镁、磷、硫和锌的试验方法
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【英文标准名称】:TestMethodforDeterminationofCalcium,Chlorine,Copper,Magnesium,Phosphorus,SulfurandZincinUnusedLubricatingOilsandAdditivesbyWavelengthDispersiveX-RayFluorescenceSpectrometry(Mathematical)
【原文标准名称】:用波长散射X射线荧光光谱法测定未用过的润滑油和添加剂中的钙、氯、铜、镁、磷、硫和锌的试验方法
【标准号】:ANSI/ASTMD6443-2004
【标准状态】:作废
【国别】:美国
【发布日期】:2004
【实施或试行日期】:2004-11-01
【发布单位】:美国国家标准学会(US-ANSI)
【起草单位】:ANSI
【标准类型】:()
【标准水平】:()
【中文主题词】:润滑油;试验方法;涡轮机油;石油工业;X射线荧光光谱法
【英文主题词】:Additives;Calcium;Chlorine;Copper;Determination;Industrialoils;Lubricants;Lubricatingoils;Magnesium;Oilindustries;Phosphorus;Sulphur;Testmethods;Testing;Turbineoils;Unused;Wavelengthdispersive;Wavelengths;X-ray;X-rayfluorescence;X-rayfluorescencespectrometry;X-rayspectrometry;Zinc
【摘要】:Thistestmethodcoversthedeterminationofcalcium,chlorine,copper,magnesium,phosphorus,sulfur,andzincinunusedlubricatingoils,additives,andadditivepackagesbywavelengthdispersiveX-rayfluorescencespectrometry.Matrixeffectsarehandledwithmathematicalcorrections.Foreachelement,theupperlimitoftheconcentrationrangecoveredbythistestmethodisdefinedbythehighestconcentrationlistedin.Samplescontaininghigherconcentrationscanbeanalyzedfollowingdilution.Foreachelement,thelowerlimitoftheconcentrationrangecoveredbythistestmethodcanbeestimatedbythelimitofdetection(LOD)(seealso40CFR136AppendixB)orlimitofquantification(LOQ),bothofwhichcanbeestimatedfromSr,therepeatabilitystandarddeviation.LODandLOQvalues,determinedfromresultsobtainedintheinterlaboratorystudyonprecision,arelistedin.LODandLOQarenotintrinsicconstantsofthistestmethod.LODandLOQdependupontheprecisionattainablebyalaboratorywhenusingthistestmethod.Thistestmethodusesregressionsoftwaretodeterminecalibrationparameters,whichcanincludeinfluencecoefficients(thatis,interelementeffectcoefficients)(GuideE1361),hereinreferencedasalphas.Alphascanalsobedeterminedfromtheoryusingrelevantsoftware.SetupofthistestmethodisintendedforpersonstrainedinthepracticeofX-rayspectrometry.Followingsetup,thistestmethodcanbeusedroutinely.ThevaluesstatedineitherSIunitsorangstromunitsaretoberegardedseparatelyasstandard.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.
【中国标准分类号】:E34
【国际标准分类号】:75_100
【页数】:
【正文语种】:英语
【原文标准名称】:用波长散射X射线荧光光谱法测定未用过的润滑油和添加剂中的钙、氯、铜、镁、磷、硫和锌的试验方法
【标准号】:ANSI/ASTMD6443-2004
【标准状态】:作废
【国别】:美国
【发布日期】:2004
【实施或试行日期】:2004-11-01
【发布单位】:美国国家标准学会(US-ANSI)
【起草单位】:ANSI
【标准类型】:()
【标准水平】:()
【中文主题词】:润滑油;试验方法;涡轮机油;石油工业;X射线荧光光谱法
【英文主题词】:Additives;Calcium;Chlorine;Copper;Determination;Industrialoils;Lubricants;Lubricatingoils;Magnesium;Oilindustries;Phosphorus;Sulphur;Testmethods;Testing;Turbineoils;Unused;Wavelengthdispersive;Wavelengths;X-ray;X-rayfluorescence;X-rayfluorescencespectrometry;X-rayspectrometry;Zinc
【摘要】:Thistestmethodcoversthedeterminationofcalcium,chlorine,copper,magnesium,phosphorus,sulfur,andzincinunusedlubricatingoils,additives,andadditivepackagesbywavelengthdispersiveX-rayfluorescencespectrometry.Matrixeffectsarehandledwithmathematicalcorrections.Foreachelement,theupperlimitoftheconcentrationrangecoveredbythistestmethodisdefinedbythehighestconcentrationlistedin.Samplescontaininghigherconcentrationscanbeanalyzedfollowingdilution.Foreachelement,thelowerlimitoftheconcentrationrangecoveredbythistestmethodcanbeestimatedbythelimitofdetection(LOD)(seealso40CFR136AppendixB)orlimitofquantification(LOQ),bothofwhichcanbeestimatedfromSr,therepeatabilitystandarddeviation.LODandLOQvalues,determinedfromresultsobtainedintheinterlaboratorystudyonprecision,arelistedin.LODandLOQarenotintrinsicconstantsofthistestmethod.LODandLOQdependupontheprecisionattainablebyalaboratorywhenusingthistestmethod.Thistestmethodusesregressionsoftwaretodeterminecalibrationparameters,whichcanincludeinfluencecoefficients(thatis,interelementeffectcoefficients)(GuideE1361),hereinreferencedasalphas.Alphascanalsobedeterminedfromtheoryusingrelevantsoftware.SetupofthistestmethodisintendedforpersonstrainedinthepracticeofX-rayspectrometry.Followingsetup,thistestmethodcanbeusedroutinely.ThevaluesstatedineitherSIunitsorangstromunitsaretoberegardedseparatelyasstandard.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.
【中国标准分类号】:E34
【国际标准分类号】:75_100
【页数】:
【正文语种】:英语
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